alpha-3-二甲基苄醇合成路线 （共 28 条）
反应条件
hydrogenchloride; calcium chloride in diethyl ether
参考文献
Lee, Ikchoon; Lee, Won Heui; Lee, Hai Whang; Bentley, T. W.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 2 p. 141 - 146
反应条件
[(2-(benzoimidazol-2-yl)-6-(3,5-dimethylpyrazol-1-yl)pyridine)RuCl2(PPh3)]; potassium tert-butylate; acetone in methanol T=56°C; Oppenauer Oxidation; P=750.075 Torr; 0.0833333 h; Inert atmosphere; Catalytic behavior;
参考文献
Wang, Qingfu; Du, Wangming; Liu, Tingting; Chai, Huining; Yu, Zhengkun
Tetrahedron Letters, 2014 , vol. 55, # 9 p. 1585 - 1588
反应条件
3 A molecular sieve; oxygen; caesium carbonate; (R)-H8-1,1'-binaphthalenyl-2,2'-diamine-based Pd(II) in toluene T=80°C; P=760 Torr; 14 h;
参考文献
Chen, Tao; Jiang, Jia-Jun; Xu, Qin; Shi, Min
Organic Letters, 2007 , vol. 9, # 5 p. 865 - 868
反应条件
potassium hydroxide; acetone; N,N'-bis[o-(diphenylphosphino)benzylidene]-(1S,2S)-diaiminocyclohexane; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in isopropyl alcohol T=25°C; 3 h;
参考文献
Stampfer, Wolfgang; Kosjek, Birgit; Faber, Kurt; Kroutil, Wolfgang
Journal of Organic Chemistry, 2003 , vol. 68, # 2 p. 402 - 406
反应条件
1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 24 h / 25 °C 2: iodine / neat (no solvent) / 2 h / 85 °C View Scheme
参考文献
Jereb, Marjan; Vrazic, Dejan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 12 p. 1978 - 1999
反应条件
T=200 - 210°C; P=120 - 130 Torr;
参考文献
Journal of the American Chemical Society, , vol. 68, p. 736
反应条件
copper oxide-chromium oxide; hydrogen T=210 - 250°C;
参考文献
Pines; Schaap
Journal of the American Chemical Society, 1958 , vol. 80, p. 3076,3079
反应条件
C53H46ClN3P2Ru; potassium isopropoxide; isopropyl alcohol
T=82°C; P=750.075 Torr; 0.0111111 h;
参考文献
Du, Wangming; Wang, Liandi; Wu, Ping; Yu, Zhengkun
Chemistry - A European Journal, 2012 , vol. 18, # 37 p. 11550 - 11554
反应条件
silver hexafluoroantimonate; (Ru2(η5-C5Ph4O)2(H)2(CO)4); Au(IPr)Cl; water in isopropyl alcohol
T=70°C; 48 h; Inert atmosphere; regioselective reaction;
参考文献
Li, Le; Herzon, Seth B.
Journal of the American Chemical Society, 2012 , vol. 134, # 42 p. 17376 - 17379,4
Title/Abstract Show Details
Li, Le; Herzon, Seth B.
Journal of the American Chemical Society, 2012 , vol. 134, # 42 p. 17376 - 17379
反应条件
potassium fluoride; dihydrogen peroxide; potassium hydrogencarbonate in tetrahydrofuran; methanol
T=20°C; 17 h;
参考文献
Yamamoto, Takeshi; Suginome, Michinori
Angewandte Chemie - International Edition, 2009 , vol. 48, # 3 p. 539 - 542
