2-(4-硝基苯基氨基)-苯甲酸合成路线 (共 12 条)
反应条件
1: phosphoryl chloride 2: SnCl2; aq.-ethanolic HCl View Scheme
参考文献
Drosdow; Drosdow
Zhurnal Obshchei Khimii, 1934 , vol. 4, p. 1
Chem. Zentralbl., 1934 , vol. 105, # II p. 3762
反应条件
copper(I) oxide; copper; potassium carbonate in 2-ethoxy-ethanol
T=130°C; 24 h;
参考文献
Mei, Xuefeng; August, Adam T.; Wolf, Christian
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 142 - 149
反应条件
potassium carbonate; CuPy2Cl2
T=75°C; 0.333333 h; microwave irradiation;
参考文献
Maradolla, Mohan Babu; Mandha, Amaravathi; Garimella, Chandra Mouli
Journal of Chemical Research, 2007 , # 10 p. 587 - 589
反应条件
potassium carbonate; CuPy2Cl2
T=75°C; 0.333333 h; microwave irradiation;
参考文献
Maradolla, Mohan Babu; Mandha, Amaravathi; Garimella, Chandra Mouli
Journal of Chemical Research, 2007 , # 10 p. 587 - 589
反应条件
1.1: palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl / toluene / 20 - 120 °C / Inert atmosphere
2.1: potassium hydroxide / ethanol; water / 20 - 100 °C / Inert atmosphere
2.2: 0 °C / pH 2 / Inert atmosphere
View Scheme
参考文献
Adeniji, Adegoke O.; Twenter, Barry M.; Byrns, Michael C.; Jin, Yi; Chen, Mo; Winkler, Jeffrey D.; Penning, Trevor M.
Journal of Medicinal Chemistry, 2012 , vol. 55, # 5 p. 2311 - 2323
反应条件
copper; potassium carbonate; nitrobenzene
参考文献
Goldberg
Chemische Berichte, 1906 , vol. 39, p. 1692
反应条件
3-methyl-1-butanol; copper
参考文献
Albert; Ritchie
Journal of the Society of Chemical Industry, London, 1941 , vol. 60, p. 121,122
Organic Syntheses, 1942 , vol. 22, p. 6
反应条件
copper(l) iodide; potassium carbonate
参考文献
Goldberg
Patent: DE185663 ;
参考文献
Pelevin; Markovich; Nazarov; Galan; Kudryavtseva; Brylev
Russian Chemical Bulletin, 2011 , vol. 60, # 3 p. 590 - 592
反应条件
1: SOCl2 / benzene / 0.5 h / Heating
2: 25percent NH4OH / 15 h / Ambient temperature
View Scheme
参考文献
Ozaki; Yamada; Oine; Ishizuka; Iwasawa
Journal of Medicinal Chemistry, 1985 , vol. 28, # 5 p. 568 - 576