反应条件
in chloroform addn. of soln. of ICl in CHCl3 to soln. of Co-compd. in CHCl3 (darkness, room temp., N2 atmosphere, 45 min); concn., pouring into ether, filtration, washing (ether), chromy. (silica gel, CH2Cl2:MeOH:pyridine 90:9:1 vol/vol);
参考文献
Inorganica Chimica Acta, , vol. 181, p. 73 - 80