potassium hydroxide; 2,3,11,12-dicyclohexano-1,4,7,10,13,16-hexaoxacyclo-octadecane in water T=110°C; 250 h; Yield given;

in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=120°C; 6 h;

1: 2-methylpropane-2-thiol With potassium hydride in tetrahydrofuran T=23°C; 0.166667 h; Inert atmosphere; 2: With zinc(II) chloride in tetrahydrofuran 0.166667 h; Inert atmosphere; 3: 1-chloro-4-bromobenzene With [P(t-Bu)3Pd(μ-Br)]2; lithium iodide in tetrahydrofuran T=90°C; 2 h; Inert atmosphere;

2,4-di-Nitrobenzene in benzene T=20°C; Addition; 24 h; Irradiation; Further byproducts given. Title compound not separated from byproducts;

in benzene-d6 Kinetics; (N2); 50°C;

in benzene-d6 Kinetics; (N2); 70°C;

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