3,3-二甲基-1-对甲苯基三氮烯合成路线 (共 8 条)
反应条件
1: With n-butyllithium in tetrahydrofuran T=0°C; 1 h; 2: With water
参考文献
Nishiwaki, Keiji; Ogawa, Takashi; Shigeta, Kazumi; Takahashi, Koichi; Matsuo, Keizo
Tetrahedron, 2006 , vol. 62, # 29 p. 7034 - 7042
反应条件
cesium fluoride in various solvent(s) T=90°C; 0.5 h; Product distribution; Further Variations:various reaction time;
参考文献
Journal of Fluorine Chemistry, , vol. 107, # 2 p. 321 - 327
反应条件
cesium fluoride in various solvent(s) T=90°C; 0.5 h; Product distribution; Further Variations:various reaction time;
参考文献
Journal of Fluorine Chemistry, , vol. 107, # 2 p. 321 - 327
反应条件
buffer solution pH 1.2 in ethanol T=37°C; μ=0.178; Rate constant;
参考文献
Nifontov, V. I.; Bel'skaya, N. P.; Chernov, V. A.; Ershova, Yu. A.; Validuda, G. I.; et al.
Pharmaceutical Chemistry Journal, 1984 , vol. 18, # 9 p. 592 - 596
Khimiko-Farmatsevticheskii Zhurnal, 1984 , vol. 18, # 9 p. 1037 - 1041
参考文献
Goldschmidt; Badl
Chemische Berichte, 1889 , vol. 22, p. 934
反应条件
1: p-toluidine With hydrogenchloride; sodium nitrite
T=0 - 10°C;
2: dimethyl amine With sodium carbonate in water
0.5 h; cooling;
参考文献
Manolov, Ilia; Machulla; Momekov
Pharmazie, 2006 , vol. 61, # 6 p. 511 - 516
参考文献
Goldschmidt; Badl
Chemische Berichte, 1889 , vol. 22, p. 934
反应条件
buffer solution pH 1.2 in ethanol
T=37°C; μ=0.178; Rate constant;
参考文献
Nifontov, V. I.; Bel'skaya, N. P.; Chernov, V. A.; Ershova, Yu. A.; Validuda, G. I.; et al.
Pharmaceutical Chemistry Journal, 1984 , vol. 18, # 9 p. 592 - 596
Khimiko-Farmatsevticheskii Zhurnal, 1984 , vol. 18, # 9 p. 1037 - 1041