in hexane byproducts: Me3SiCl; under protective gas; solution of 1 equivalent Si-compound and 2 equivalents B-compound was refluxed for 1 h; cooling;; precipitate was separated, washed (hexane/CH2Cl2) and dried (vacuo); filtrate contains B(NMe2)3; elem. anal.;;

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S4N5Cl in acetonitrile 1) -45 deg C, 2) to 10 deg C, 1 h;