乙基3-羟基-2-萘甲酸酯合成路线 (共 13 条)
反应条件
ammonia T=170°C; im geschlossenen Rohr;
参考文献
Bucherer; Seyde
Journal fuer Praktische Chemie (Leipzig), 1907 , vol. <2> 75, p. 288
参考文献
Rai, Ganesha; Kenyon, Victor; Jadhav, Ajit; Schultz, Lena; Armstrong, Michelle; Jameson, J. Brian; Hoobler, Eric; Leister, William; Simeonov, Anton; Holman, Theodore R.; Maloney, David J.
Journal of Medicinal Chemistry, 2010 , vol. 53, # 20 p. 7392 - 7404
反应条件
dipotassium peroxodisulfate; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; trifluoroacetic acid; trifluoroacetic anhydride
T=100°C; 11 h;
参考文献
Yang, Yiqing; Lin, Yun; Rao, Yu
Organic Letters, 2012 , vol. 14, # 11 p. 2874 - 2877
参考文献
Oshima; Hayashi
Kogyo Kagaku Zasshi, 1941 , vol. 44, p. 821
Chem.Abstr., 1948 , p. 2108
反应条件
1: thionyl chloride / CH2Cl2 / 3 h
2: Et3N / CH2Cl2 / 6 h / Heating
View Scheme
参考文献
Franczyk, Thaddeus S.; Czerwinski, Kenneth R.; Raymond, Kenneth N.
Journal of the American Chemical Society, 1992 , vol. 114, # 21 p. 8138 - 8146
反应条件
sodium hydrogencarbonate; 1-n-butyl-3-methylimidazolium hexafluorophosphate
T=40°C; 0.416667 h;
参考文献
Ambika; Singh, Pradeep Pratap; Chauhan
Synthetic Communications, 2008 , vol. 38, # 6 p. 928 - 936
参考文献
Palmer,M.H.; Scollick,N.M.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 2836 - 2841
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Rosenberg
Chemische Berichte, 1892 , vol. 25, p. 3635
反应条件
palladium diacetate; caesium carbonate; 2-dicyclohexylphosphino-1,1'-biphenyl in toluene
T=100°C;
参考文献
Xie, Fuchun; Li, Bingbing X.; Xiao, Xiangshu
Letters in Organic Chemistry, 2013 , vol. 10, # 5 p. 380 - 384
参考文献
Sieger et al.
Journal of the American Pharmaceutical Association (1912-1977), 1958 , vol. 47, p. 734,738
参考文献
Cohen et al.
British Journal of Pharmacology and Chemotherapy, 1957 , vol. 12, p. 194,206