2-(甲基硫代)苯并咪唑合成路线 (共 30 条)
反应条件
2,4,6-trichloro-1,3,5-triazine; potassium iodide in acetonitrile T=20°C; 0.25 h; chemoselective reaction;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad M.; Sohrabnezhad, Samira
Tetrahedron Letters, 2011 , vol. 52, # 48 p. 6420 - 6423
反应条件
N-ethyl-N,N-diisopropylamine in acetone T=20°C; 0.0166667 h; Sonication;
参考文献
Deligeorgiev, Todor; Kaloyanova, Stefka; Lesev, Nedyalko; Vaquero, Juan J.
Ultrasonics Sonochemistry, 2010 , vol. 17, # 5 p. 783 - 788
反应条件
triethylamine in tetrahydrofuran
参考文献
Gardiner, John M.; Loyns, Colin R.
Tetrahedron, 1995 , vol. 51, # 42 p. 11515 - 11530
反应条件
potassium tert-butylate; oxygen; dimethyl sulfoxide T=25°C; 0.0833333 h;
参考文献
Haddach, Aubrey A.; Kelleman, Audrey; Deaton-Rewolinski, Melissa V.
Tetrahedron Letters, 2002 , vol. 43, # 3 p. 399 - 402
反应条件
sodium hydroxide; Amberlite IRA-400 chloride form in water; acetone
参考文献
Dalal; Pawar; Mahulikar
Organic Preparations and Procedures International, 2005 , vol. 37, # 6 p. 539 - 546
反应条件
in water T=60°C; 1 h; Heating;
参考文献
Heterocycles, , vol. 55, # 1 p. 45 - 58
反应条件
hydrogenchloride 2 h; Heating;
参考文献
Abramova, N. D.; Skvortsova, G. G.; Trzhtsinskaya, B. V.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 1854
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 9 p. 2031 - 2032
反应条件
in toluene 0.05 h; Heating;
参考文献
Stanovnik, Branko; Tisler, Miha; Hribar, Alenka; Barlin, Gordon B.; Brown, Desmond J.
Australian Journal of Chemistry, 1981 , vol. 34, # 8 p. 1729 - 1738
反应条件
1: tetrahydrofuran / 0.08 h / 20 °C 2: LDA / 1.) THF, -20 deg C, 60 min, 2.) from -78 deg C to 20 deg C, 8 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 54, # 12 p. 2949 - 2952
反应条件
1-n-butyl-3-methylimidazolium chloride T=110°C; 6 h; regioselective reaction;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 186, # 1 p. 31 - 37