thermal decomp. between 25 and 100 °C and dynamic vacuum to remove HF; determination of distribution of (18)F;

thermal decomp. between 25 and 100 °C and dynamic vacuum to remove HF; determination of distribution of (18)F;

in neat (no solvent) byproducts: NF3, HF; TeF5OH was added to NF4NF2*99HF on vac. line at -196°C, warmed slowly to -23°C, kept for 8 h under dynamic vac.; volatiles sepd. by fractional condensation in traps (-95, -126, -142 and -210°C);

thermal decomp. between 25 and 100 °C and dynamic vacuum to remove HF; determination of distribution of (18)F;