Alpha-乙氧草酰基苯乙酸乙酯合成路线 （共 11 条）
反应条件
1: 20 - 40 Torr / bei der Destillation 2: water; alcoholic sodium ethylate 3: beim Schmelzen View Scheme
参考文献
Malki, Fatiha; Touati, Abdelkader; Rahal, Said; Moulay, Saad
Asian Journal of Chemistry, 2011 , vol. 23, # 3 p. 961 - 967
反应条件
T=170 - 180°C; 12 h;
参考文献
Malki, Fatiha; Touati, Abdelkader; Rahal, Said; Moulay, Saad
Asian Journal of Chemistry, 2011 , vol. 23, # 3 p. 961 - 967
参考文献
Wislicenus,W.
Chemische Berichte, 1887 , vol. 20, p. 592
Justus Liebigs Annalen der Chemie, 1888 , vol. 246, p. 340
反应条件
1: 20 - 40 Torr / bei der Destillation 2: water; alcoholic sodium ethylate View Scheme
参考文献
Malki, Fatiha; Touati, Abdelkader; Rahal, Said; Moulay, Saad
Asian Journal of Chemistry, 2011 , vol. 23, # 3 p. 961 - 967
反应条件
potassium carbonate in water
参考文献
Jefford, Charles W.; Zaslona, Alexander
Tetrahedron Letters, 1985 , vol. 26, # 49 p. 6035 - 6038
反应条件
ethanol; sodium in ethanol
48 h; Ambient temperature;
参考文献
Jefford, Charles W.; Kubota, Tadatoshi; Zaslona, Alexander
Helvetica Chimica Acta, 1986 , vol. 69, p. 2048 - 2061
反应条件
diethyl ether; sodium ethanolate
Eintragen von Phenylessigsaeureaethylester; man zersetzt die erhaltene Natriumverbindung mit verd. Schwefelsaeure;
参考文献
Wislicenus,W.
Chemische Berichte, 1894 , vol. 27, p. 1092
反应条件
1: sulfuric acid; water
2: sodium ethanolate
View Scheme
参考文献
Malki, Fatiha; Touati, Abdelkader; Rahal, Said; Moulay, Saad
Asian Journal of Chemistry, 2011 , vol. 23, # 3 p. 961 - 967
反应条件
man saeuert mit verd. Schwefelsaeure an;
参考文献
Wislicenus,W.
Chemische Berichte, 1887 , vol. 20, p. 592
Justus Liebigs Annalen der Chemie, 1888 , vol. 246, p. 340
反应条件
1: 12 h / 170 - 180 °C
2: water; potassium hydroxide / 51 - 73 °C
3: phosphorus pentachloride / dichloromethane / 2 h / 20 °C
4: pyridine / dichloromethane / 20 °C
View Scheme
参考文献
Malki, Fatiha; Touati, Abdelkader; Rahal, Said; Moulay, Saad
Asian Journal of Chemistry, 2011 , vol. 23, # 3 p. 961 - 967
