1-(2,4-二硝基苯基)-4,4'-联吡啶鎓二氯化物合成路线 (共 4 条)
反应条件
T=150 - 170°C; Zincke reaction; neat (no solvent);
参考文献
Deligkiozi, Ioanna; Papadakis, Raffaello; Tsolomitis, Athanase
Supramolecular Chemistry, 2012 , vol. 24, # 5 p. 333 - 343
反应条件
in acetone
Condensation; 15 h; Heating;
参考文献
Nimkar, Sandeep K.; Anderson, Andrea H.; Rimoldi, John M.; Stanton, Matthew; Castagnoli, Kay P.; Mabic, Stephane; Wang; Castagnoli Jr., Neal
Chemical Research in Toxicology, 1996 , vol. 9, # 6 p. 1013 - 1022
反应条件
in ethylene glycol
T=120°C; 6 h; Product distribution / selectivity;
参考文献
FUJI PHOTO FILM CO., LTD.
Patent: WO2005/95342 A1, 2005 ;
Location in patent: Page/Page column 26-27 ;
反应条件
in water
5 h; Inert atmosphereReflux;
参考文献
Zhang, Kang-Da; Tian, Jia; Hanifi, David; Zhang, Yuebiao; Sue, Andrew Chi-Hau; Zhou, Tian-You; Zhang, Lei; Zhao, Xin; Liu, Yi; Li, Zhan-Ting
Journal of the American Chemical Society, 2013 , vol. 135, # 47 p. 17913 - 17918