2-(溴甲基)苯甲酸乙酯合成路线 (共 38 条)
反应条件
1: toluene / 20 °C
2: triethylamine / chloroform; methanol / 12 h / 20 °C
View Scheme
参考文献
Kadam, Hari K.; Tilve, Santosh G.
European Journal of Organic Chemistry, 2013 , # 20 p. 4280 - 4284
反应条件
bis(cyclopentadienyl)titanium dichloride; zinc in tetrahydrofuran
T=20°C; radical induced Barbier-type reaction;
参考文献
Mandal, Samir Kumar; Roy, Subhas Chandra
Tetrahedron, 2008 , vol. 64, # 49 p. 11050 - 11057
反应条件
1: dimethylformamide / 60 °C
2: formic acid; concentrated sulfuric acid
View Scheme
参考文献
Bornstein et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 83,85
参考文献
Kadam, Hari K.; Tilve, Santosh G.
European Journal of Organic Chemistry, 2013 , # 20 p. 4280 - 4284
反应条件
potassium carbonate in acetone
T=20°C;
参考文献
Prasad, Chalasani S.N.; Varala, Ravi; Adapa, Srinivas R.
Heterocyclic Communications, 2002 , vol. 8, # 3 p. 281 - 286
参考文献
Davies; Perkin
Journal of the Chemical Society, 1922 , vol. 121, p. 2213
参考文献
Davies; Perkin
Journal of the Chemical Society, 1922 , vol. 121, p. 2213
反应条件
bis(cyclopentadienyl)titanium dichloride; zinc in tetrahydrofuran
T=20°C; radical induced Barbier-type reaction;
参考文献
Mandal, Samir Kumar; Roy, Subhas Chandra
Tetrahedron, 2008 , vol. 64, # 49 p. 11050 - 11057