2-(溴甲基)苯甲酸乙酯合成路线 （共 38 条）
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane T=0°C; 3.5 h; Heating / reflux;
参考文献
DarPharma, Inc.
Patent: US2007/155720 A1, 2007 ;
Location in patent: Page/Page column 22 ;
US 20070155720 A1
反应条件
1: 89 percent / H2SO4 2: 84 percent / NBS / CCl4 View Scheme
参考文献
Synthetic Communications, , vol. 34, # 4 p. 579 - 588
反应条件
1: SOCl2 View Scheme
参考文献
Tetrahedron, , vol. 22, p. 2107 - 2117
反应条件
1: 2.) H2 / 1.) Ra Ni, 2.) 5percent Rh/C / 1.) EtOH, RT, 0.5 h, 2.) MeOH, 6 h 2: N-bromosuccinimide (NBS) / CCl4 / 18 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 12 p. 2128 - 2133
参考文献
Jung, Michael E.; Lam, Patrick Yuk-Sun; Mansuri, Muzzamil M.; Speltz, Laurine M.
Journal of Organic Chemistry, 1985 , vol. 50, # 7 p. 1087 - 1105
反应条件
N-bromosuccinmide in tetrachloromethane 18 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 50, # 12 p. 2128 - 2133
反应条件
in diethyl ether 11 h;
参考文献
Journal of Organic Chemistry, , vol. 54, # 17 p. 4253 - 4256
参考文献
Tetrahedron, , vol. 22, p. 2107 - 2117
参考文献
Journal of the Chemical Society, , vol. 121, p. 2213
反应条件
1: 90 percent / potassium carbonate / acetone / 20 °C 2: 88 percent / sodium borohydride / methanol / 1 h 3: 66 percent / conc. HCl / CHCl3 4: 51.6 percent / triphenyl phosphine; sodium acetate; triethylbenzylammonium chloride / Pd(PPh3)2Cl2 / 20 h / 90 °C 5: 40 percent / aq. KOH / 1 h / Heating View Scheme
参考文献
Prasad, Chalasani S.N.; Varala, Ravi; Adapa, Srinivas R.
Heterocyclic Communications, 2002 , vol. 8, # 3 p. 281 - 286
