顺式-环丙烷-1,2-二羧酸二乙酯合成路线 (共 16 条)
反应条件
sodium hydride in toluene T=60°C; 1 h; to initiate the reaction MeOH;
参考文献
Tetrahedron, , vol. 50, # 35 p. 10431 - 10442
反应条件
4-(N,N-dimethlyamino)pyridine in chlorobenzene T=20°C; 20 h; Title compound not separated from byproducts.;
参考文献
Journal of the American Chemical Society, , vol. 129, # 40 p. 12074 - 12075
参考文献
Journal of Organic Chemistry, , vol. 32, p. 3351 - 3355
反应条件
sulfuric acid 5 h; Heating;
参考文献
Majchrzak, Michal W.; Kotelko, Antoni; Lambert, Joseph B.
Synthesis, 1983 , # 6 p. 469 - 470
参考文献
Journal of Organic Chemistry, , vol. 29, p. 1249 - 1251
反应条件
2: aq. HCl View Scheme
参考文献
Journal of Organic Chemistry, , vol. 29, p. 1249 - 1251
反应条件
1: 1.) aq. NaOH, 2.) acetic anhydride / 1.) 15 h, reflux, 2.) 0.5 h, reflux 2: 70 percent / sulfuric acid / 5 h / Heating View Scheme
参考文献
Synthesis, , # 6 p. 469 - 470
反应条件
1: 1.) aq. NaOH, 2.) acetic anhydride / 1.) 15 h, reflux, 2.) 0.5 h, reflux 2: 70 percent / sulfuric acid / 5 h / Heating View Scheme
参考文献
Synthesis, , # 6 p. 469 - 470
参考文献
Helvetica Chimica Acta, , vol. 12, p. 1153
反应条件
sodium hydride 1.) DMSO, 20 min, 2.) 1 h; Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 12 p. 2921 - 2926