1: propan-1-ol; carbon dioxide With 1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
T=-42°C; 0.75 h;
2: trifluoromethanesulfonic anhydride in acetonitrile
T=-20°C; 0.666667 h; Title compound not separated from byproducts;
参考文献
Bratt, Mark O.; Taylor, Paul C.
Journal of Organic Chemistry, 2003 , vol. 68, # 14 p. 5439 - 5444
(i) HCO2H, (ii) /BRN= 1098242/; Multistep reaction;
参考文献
Evdakov,V.P.; Mizrakh,L.I.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, p. 1848 - 1851,1860 - 1862
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Evdakov,V.P.; Alipova,E.I.
J. Gen. Chem. USSR (Engl. Transl.), 1965 , vol. 35, p. 1584 - 1587,1588 - 1590