2-(4-溴苯基)-2-氧代乙酸合成路线 （共 24 条）
反应条件
(R)-ketoacid reductase from Saccharomyces cerevisiae ZJB5074; glycerol in aq. phosphate buffer T=30°C; pH=7.5; Enzymatic reaction; enantioselective reaction;
参考文献
Xue, Ya-Ping; Zheng, Yu-Guo; Zhang, Ya-Qin; Sun, Jing-Lei; Liu, Zhi-Qiang; Shen, Yin-Chu
Chemical Communications, 2013 , vol. 49, # 91 p. 10706 - 10708
反应条件
dipotassium peroxodisulfate; palladium diacetate in water; dimethyl sulfoxide T=20°C; 3 h;
参考文献
Li, Mingzong; Wang, Cong; Ge, Haibo
Organic Letters, 2011 , vol. 13, # 8 p. 2062 - 2064
反应条件
palladium (II) trifluoroacetate; silver carbonate in ethylene glycol dimethyl ether T=130°C; 24 h; Sealed tube; chemoselective reaction;
参考文献
Miao, Jinmin; Ge, Haibo
Organic Letters, 2013 , vol. 15, # 12 p. 2930 - 2933
反应条件
Ru(phen)3(Cl)2; oxygen in dimethyl sulfoxide T=32°C; 36 h; IrradiationSchlenk technique;
参考文献
Liu, Jie; Liu, Qiang; Yi, Hong; Qin, Chu; Bai, Ruopeng; Qi, Xiaotian; Lan, Yu; Lei, Aiwen
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 502 - 506
Angew. Chem., 2014 , vol. 126, # 2 p. 512 - 516,5
反应条件
water in acetonitrile T=25°C; Decarboxylation; Irradiation; Quantum yield; Further Variations:SolventspH-valuesλ&irr%;
参考文献
Goerner, Helmut; Kuhn, Hans Jochen
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 12 p. 2671 - 2680
反应条件
Ru(phen)3(Cl)2; oxygen in dimethyl sulfoxide T=32°C; 36 h; IrradiationSchlenk technique;
参考文献
Liu, Jie; Liu, Qiang; Yi, Hong; Qin, Chu; Bai, Ruopeng; Qi, Xiaotian; Lan, Yu; Lei, Aiwen
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 502 - 506
Angew. Chem., 2014 , vol. 126, # 2 p. 512 - 516,5
反应条件
1: in water; dimethyl sulfoxide T=100°C; 1 h; Inert atmosphere; 2: With dipotassium peroxodisulfate 3 h; Inert atmosphere;
参考文献
Yang, Zhiyong; Chen, Xiang; Wang, Sizhuo; Liu, Jidan; Xie, Kai; Wang, Anwei; Tan, Ze
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 7086 - 7091
反应条件
sulfuric acid in benzene
参考文献
Adlerova,E. et al.
Collection of Czechoslovak Chemical Communications, 1964 , vol. 29, p. 97 - 120
反应条件
selenium(IV) oxide in 1,4-dioxane
2 h; Reflux;
参考文献
Nagaraj, Muthupandi; Perumal, Devanathan; Boominathan, Muthusamy; Muthusubramanian, Shanmugam; Bhuvanesh, Nattamai
Journal of Sulfur Chemistry, 2014 , vol. 35, # 1 p. 24 - 30
反应条件
selenium(IV) oxide in pyridine
T=90 - 110°C; Schlenk technique;
参考文献
Liu, Jie; Liu, Qiang; Yi, Hong; Qin, Chu; Bai, Ruopeng; Qi, Xiaotian; Lan, Yu; Lei, Aiwen
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 502 - 506
Angew. Chem., 2014 , vol. 126, # 2 p. 512 - 516,5
