7-(3-溴丙氧基)-3,4-二氢喹啉-2(1H)-酮合成路线 (共 3 条)
反应条件
1: 6-hydroxy-1,2,3,4-tetrahydro-2-quinolinone With potassium carbonate in water; acetone
T=20°C; 1 h;
2: 1,3-dibromo-propane in water; acetone
T=20°C; 16 h;
参考文献
Pai; Samel
Asian Journal of Chemistry, 2011 , vol. 23, # 4 p. 1655 - 1660
反应条件
1.1: AlCl3, aluminium chloride / N,N-dimethyl acetamide / 140 - 150 °C
2.1: potassium carbonate / water; acetone / 1 h / 20 °C
2.2: 16 h / 20 °C
View Scheme
参考文献
Pai; Samel
Asian Journal of Chemistry, 2011 , vol. 23, # 4 p. 1655 - 1660
反应条件
1.1: sodium carbonate / toluene / 2 h / 40 - 65 °C
2.1: AlCl3, aluminium chloride / N,N-dimethyl acetamide / 140 - 150 °C
3.1: potassium carbonate / water; acetone / 1 h / 20 °C
3.2: 16 h / 20 °C
View Scheme
参考文献
Pai; Samel
Asian Journal of Chemistry, 2011 , vol. 23, # 4 p. 1655 - 1660