3,3-二甲基1,5-二氧杂螺[5.5]十一烷合成路线 （共 14 条）
反应条件
water in acetone T=20 - 55°C;
参考文献
Verma, Sanjeev K.; Sathe, Manisha; Kaushik
Synthetic Communications, 2010 , vol. 40, # 11 p. 1701 - 1707
反应条件
T=30°C; Equilibrium constant;
参考文献
Newman; Harper
Journal of the American Chemical Society, 1958 , vol. 80, p. 6350,6353
反应条件
T=30°C; Equilibrium constant;
参考文献
Journal of the American Chemical Society, , vol. 80, p. 6350,6353
反应条件
indium trifluoromethanesulfonate in dichloromethane
T=20°C; 0.5 h;
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.
Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
反应条件
indium trifluoromethanesulfonate
T=20°C; 0.5 h; Neat (no solvent);
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.
Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
反应条件
N-(4-methyoxybenzyl)-2-cyanopyridinium hexafluoroantimonate in toluene
1.5 h; Heating;
参考文献
Lee; Takata; Endo
Synthesis, 1991 , # 5 p. 368 - 370
反应条件
toluene-4-sulfonic acid in dichloromethane
T=20°C; 0.5 h; chemoselective reaction;
参考文献
Rahimizadeh, Mohammad; Bakavoli, Mehdi; Shiri, Ali; Eshghi, Hossein; Saberi, Sattar
Journal of Chemical Research, 2008 , # 12 p. 704 - 706
反应条件
toluene-4-sulfonic acid in n-heptane
T=20°C; Condensation; 1.5 h;
参考文献
Gvozdik; Gal'chenko; Musavirov
Russian Journal of General Chemistry, 1996 , vol. 66, # 5 p. 784 - 787
反应条件
1: 68 percent / toluene / 0.25 h
2: 60 percent / para-toluenesulfonic acid / heptane / 1.5 h / 20 °C
View Scheme
参考文献
Gvozdik; Gal'chenko; Musavirov
Russian Journal of General Chemistry, 1996 , vol. 66, # 5 p. 784 - 787
反应条件
1: indium trifluoromethanesulfonate / dichloromethane / 20 °C
2: indium trifluoromethanesulfonate / 0.5 h / 20 °C / Neat (no solvent)
View Scheme
参考文献
Smith, Brendan M.; Kubczyk, Tomasz M.; Graham, Andrew E.
Tetrahedron, 2012 , vol. 68, # 38 p. 7775 - 7781
