in tetrahydrofuran Irradiation (UV/VIS); Stirring of nitroso compound in THF under N2, metal carbonyl in THF is added, the soln. is irradiated (sunlamp photolysis) for a period of 3 h at 30°C.; final purifn. by chromy. on silica gel, elution with 19/1 hexane/ethyl acetate provides a single compound;
参考文献
Journal of Organometallic Chemistry, , vol. 368, p. 83 - 102