Alpha-(1-甲基乙基)苯乙醇合成路线 (共 32 条)
反应条件
chromium(VI) oxide - pyridine in dichloromethane
参考文献
Barentsen, Helma M.; Sieval, Alex B.; Cornelisse, Jan
Tetrahedron, 1995 , vol. 51, # 27 p. 7495 - 7520
参考文献
Levy
Bulletin de la Societe Chimique de France, 1923 , vol. <4> 33, p. 1662
反应条件
n-butyllithium in tetrahydrofuran
T=-78°C; 0.0333333 h;
参考文献
Sawyer,J.S.; Kucerovy,A.; Macdonald,T.L.
Journal of the American Chemical Society, 1988 , vol. 110, p. 842
反应条件
cyclohexanone in tetrahydrofuran
under argon; treatment of tin-compound in THF at -78 °C with LiBu; stirring 2 min; quenching with cyclohexanone;; poured into NH4Cl-soln. and petroleum ether; shaked 1 min; org. layer separated, washed (brine), dried (Na2SO4), filtered, concd. (vacuo); chromd. (silica gel; ethyl acetate/ petroleum ether 10:90); identical with substance produced otherwise;;
参考文献
Sawyer,J.S.; Kucerovy,A.; Macdonald,T.L.
Journal of the American Chemical Society, 1988 , vol. 110, p. 842
反应条件
lithium in tetrahydrofuran
T=-30°C; 0.25 h;
参考文献
Guijarro, David; Mancheno, Balbino; Yus, Miguel
Tetrahedron, 1994 , vol. 50, # 28 p. 8551 - 8558
反应条件
naphthalene; lithium in tetrahydrofuran
T=-78 - 20°C; 5 h;
参考文献
Alonso, Emma; Guijarro, David; Yus, Miguel
Tetrahedron, 1995 , vol. 51, # 9 p. 2699 - 2708
反应条件
naphthalene; lithium in tetrahydrofuran
T=-78 - 0°C; 2 h;
参考文献
Alonso, Emma; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 1996 , vol. 52, # 45 p. 14341 - 14348
反应条件
4,4'-di-tert-butylbiphenyl; lithium in tetrahydrofuran
T=-78 - 20°C; 4 h;
参考文献
Guijarro; Yus
Tetrahedron, 1994 , vol. 50, # 11 p. 3447 - 3452
反应条件
naphthalene; lithium in tetrahydrofuran
T=0°C; 2 h;
参考文献
Guijarro, D.; Mancheno, B.; Yus, M.
Tetrahedron, 1992 , vol. 48, # 22 p. 4593 - 4600
反应条件
naphthalene; lithium in tetrahydrofuran
T=-30°C; Condensation; 2 h;
参考文献
Alonso, Emma; Guijarro, David; Martinez, Pedro; Ramon, Diego J.; Yus, Miguel
Tetrahedron, 1999 , vol. 55, # 36 p. 11027 - 11038