(S)-(+)-2-氯-1-苯乙醇合成路线 (共 6 条)
反应条件
sodium hydroxide T=20°C; 2 h;
参考文献
Wei, Shengwei; Messerer, Regina; Tsogoeva, Svetlana B.
Chemistry - A European Journal, 2011 , vol. 17, # 51 p. 14380 - 14384
反应条件
(Ru2(η5-C5Ph4O)2(H)2(CO)4); potassium tert-butylate in toluene T=80°C; 29 h; Reactivity; Reagent/catalystTime;
参考文献
Journal of the American Chemical Society, , vol. 130, # 41 p. 13508 - 13509
反应条件
ammonium hydroxide in methanol; water T=20°C;
参考文献
Tanielyan, Setrak K.; Marin, Norman; Alvez, Gabriela; Augustine, Robert L.
Organic Process Research and Development, 2006 , vol. 10, # 5 p. 893 - 898
反应条件
chlorodicarbonyl(1-(isopropylamino)-2,3,4,5-tetraphenylcyclopentadienyl) ruthenium(II); potassium tert-butylate in toluene T=20°C; 0.5 h; Inert atmosphere; Reactivity; Reagent/catalystTemperatureTimeSolvent;
参考文献
Mutti, Francesco G.; Orthaber, Andreas; Schrittwieser, Joerg H.; Vries, Johannes G. De; Pietschnig, Rudolf; Kroutil, Wolfgang
Chemical Communications, 2010 , vol. 46, # 42 p. 8046 - 8048
反应条件
(Ru2(η5-C5Ph4O)2(H)2(CO)4); potassium tert-butylate in toluene T=80°C; 29 h; Reactivity; Reagent/catalystTime;
参考文献
Haak, Robert M.; Berthiol, Florian; Jerphagnon, Thomas; Gayet, Arnaud J. A.; Tarabiono, Chiara; Postema, Christiaan P.; Ritleng, Vincent; Pfeffer, Michel; Janssen, Dick B.; Minnaard, Adriaan J.; Feringa, Ben L.; De Vries, Johannes G.
Journal of the American Chemical Society, 2008 , vol. 130, # 41 p. 13508 - 13509
反应条件
1: (R)-(+)-2-chloro-1-phenylethyl alcohol With [Ir(η5-C5Me5)(C6H4-2-CH2NHCH3)(NCCH3)](PF6); potassium tert-butylate in toluene T=20°C; 16 h; Inert atmosphere; 2: (S)-2-chloro-1-phenylethanol in toluene T=20°C; 2 h; Inert atmosphere;
参考文献
Jerphagnon, Thomas; Gayet, Arnaud J.A.; Berthiol, Florian; Ritleng, Vincent; Mrsic, Natasa; Meetsma, Auke; Pfeffer, Michel; Minnaard, Adriaan J.; Feringa, Ben L.; De Vries, Johannes G.
Chemistry - A European Journal, 2009 , vol. 15, # 46 p. 12780 - 12790