(4-甲氧基苯基)-二甲胺合成路线 (共 83 条)
反应条件
ruthenium trichloride; oxygen; acetic acid in methanol T=60°C; P=760.051 Torr; 4 h;
参考文献
Murahashi, Shun-Ichi; Nakae, Takahiro; Terai, Hiroyuki; Komiya, Naruyoshi
Journal of the American Chemical Society, 2008 , vol. 130, # 33 p. 11005 - 11012
反应条件
ruthenium trichloride; oxygen; acetic acid in methanol T=60°C; P=760 Torr;
参考文献
Murahashi, Shun-Ichi; Komiya, Naruyoshi; Terai, Hiroyuki
Angewandte Chemie - International Edition, 2005 , vol. 44, # 42 p. 6931 - 6933
反应条件
tert.-butylhydroperoxide; iron(II) chloride in methanol; decane T=20°C; Inert atmosphere;
参考文献
Han, Wei; Ofial, Armin R.
Chemical Communications, 2009 , # 33 p. 5024 - 5026
反应条件
oxygen; iron(III) chloride in acetonitrile T=50°C; P=760 Torr; 16 h;
参考文献
Murata, Satoru; Teramoto, Koji; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 4 p. 1297 - 1298
反应条件
Benzoyl cyanide; oxygen; iron(III) chloride in acetonitrile T=50°C; P=760 Torr; 16 h;
参考文献
Murata, Satoru; Teramoto, Koji; Miura, Masahiro; Nomura, Masakatsu
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 4 p. 1297 - 1298
反应条件
1: 1.) NH3 liq., Li, 2.) NaCNBH3, HCl / 1.) MeOH, THF, -35 deg C, 20 min, 2.) THF, 0 deg C, 1 h 2: 75 percent / HCl / Heating 3: 50 percent / 2M aq. HCl / diethyl ether / 5 h / Ambient temperature View Scheme
参考文献
Stanetty, Peter; Kasemann, Olaf; Schmid, Martin
Journal of Chemical Research, Miniprint, 1995 , # 9 p. 2101 - 2110
反应条件
1: N,N-dimethyl-formamide / 20 °C / |Inert atmosphere; |Schlenk technique 2: C27H22Cl2N3NiP / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 12 h / |Inert atmosphere; |Schlenk technique; |Heating View Scheme
参考文献
Zhang, Qiang; Zhang, Xue-Qi; Wang, Zhong-Xia
Dalton Transactions, 2012 , vol. 41, # 34 p. 10453 - 10464,12
反应条件
alpha,alpha-dimethylbenzyl hydroperoxide; C-40 bovine liver catalase T=25°C; 0.0833333 h; 0.1 M NaH2PO4-Na2HPO4 ( pH = 7.4 ); Rate constantProduct distribution;
参考文献
Sayo, Hiroteru; Hosokawa, Mikio
Chemical & Pharmaceutical Bulletin, 1985 , vol. 33, # 10 p. 4471 - 4477
反应条件
1: dichloromethane / 4 h / 20 °C / Inert atmosphere 2: Ni(PCy3)2Cl2 / tetrahydrofuran; 1-methyl-pyrrolidin-2-one / 8 h / 90 °C / Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 21 p. 4901 - 4904
反应条件
in pentane T=-80.15°C; Kinetics; Further Variations:Solvents;
参考文献
Fukuzumi, Shunichi; Shimoosako, Kanji; Suenobu, Tomoyoshi; Watanabe, Yoshihito
Journal of the American Chemical Society, 2003 , vol. 125, # 30 p. 9074 - 9082