2-羟基-6-甲氧基苯甲醛合成路线 (共 48 条)
反应条件
methyl-3-phenyl-2-propynoate; cesium fluoride T=25°C; 1 h; Inert atmosphere; Reagent/catalyst;
参考文献
Tetrahedron Letters, , vol. 55, # 8 p. 1402 - 1405
反应条件
aluminium trichloride; sodium iodide in dichloromethane; acetonitrile 0.75 h; Ambient temperature;
参考文献
Heterocycles, , vol. 39, # 2 p. 613 - 622
反应条件
lithium chloride in N,N-dimethyl-formamide T=75°C; 6 h;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 19 p. 2925 - 2929
反应条件
diisobutylaluminium hydride in tetrahydrofuran T=-78°C;
参考文献
Journal of Molecular Catalysis B: Enzymatic, , vol. 66, # 3-4 p. 276 - 284
反应条件
1: With AlCl3, aluminium chloride in dichloromethane T=-15 - 20°C; 5 h; Inert atmosphereLarge scale; 2: With hydrogenchloride in dichloromethane; water T=25°C; Inert atmosphereLarge scale;
参考文献
Organic Process Research and Development, , vol. 8, # 6 p. 897 - 902
反应条件
1: 3-methoxy-phenol With n-butyllithium in hexane; dichloromethane T=20°C; 12 h; 2: N-methyl-N-formyl-aniline in diethyl ether; hexane; dichloromethane 0.5 h; Heating;
参考文献
Helvetica Chimica Acta, , vol. 85, # 2 p. 442 - 450
反应条件
triethylamine; magnesium chloride in acetonitrile 2 h; Heating;
参考文献
Acta Chemica Scandinavica, , vol. 53, # 4 p. 258 - 262
反应条件
1: N,N-dimethyl-formamide; 3-methoxy-2-(trimethylsilyl)phenyl-trifluoromethanesulfonate With cesium fluoride T=20°C; 0.25 h; Inert atmosphere; 2: triethyl borane T=20°C; 12 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 12, # 9 p. 1956 - 1959
反应条件
potassium carbonate in N,N-dimethyl-formamide
参考文献
Journal of Medicinal Chemistry, , vol. 22, # 9 p. 1082 - 1088