1-(2-羟基-3-甲基-苯基)-乙酮合成路线 （共 31 条）
反应条件
1: sodium acetate / Destillieren des Reaktionsgemisches unter vermindertem Druck; Behandeln mit Soda 2: NaOH-solution View Scheme
参考文献
Wittig
Justus Liebigs Annalen der Chemie, 1926 , vol. 446, p. 179
反应条件
n-butyllithium; gallium(II) chloride in chlorobenzene
T=80°C; 3 h;
参考文献
Kobayashi, Katsumi; Arisawa, Mieko; Yamaguchi, Masahiko
Journal of the American Chemical Society, 2002 , vol. 124, # 29 p. 8528 - 8529
反应条件
1: ortho-cresol With n-butyllithium; gallium(II) chloride in hexane; chlorobenzene
T=20°C; 0.166667 h;
2: 1-chloro-2-(trimethylsilyl)ethyne With 2,6-di-tert-butyl-4-methylpyridine in hexane; chlorobenzene
Further stages.;
参考文献
Kobayashi, Katsumi; Arisawa, Mieko; Yamaguchi, Masahiko
Journal of the American Chemical Society, 2002 , vol. 124, # 29 p. 8528 - 8529
反应条件
aluminum oxide; methanesulfonic acid
T=160°C; 0.166667 h;
参考文献
Sharghi, Hashem; Kaboudin, Babak
Journal of Chemical Research, Miniprint, 1998 , # 10 p. 2678 - 2695
反应条件
N,N-dimethyl-formamide; zinc
T=68°C; Fries rearrangement; 0.5 h;
参考文献
Paul, Satya; Gupta, Monika
Synthesis, 2004 , # 11 p. 1789 - 1792
反应条件
aluminum oxide; methanesulfonic acid
T=140°C; 5 h;
参考文献
Sharghi, Hashem; Kaboudin, Babak
Journal of Chemical Research, Miniprint, 1998 , # 10 p. 2678 - 2695
反应条件
iodine; 1-(2-hydroxy-3-methyl-phenacyl)-pyridinium; iodide
参考文献
King; McWhirter; Barton
Journal of the American Chemical Society, 1945 , vol. 67, p. 2089,2090
反应条件
boron trifluoride diethyl etherate
0.0333333 h; microwave irradiation;
参考文献
Naeimi, Hossein; Moradi, Leila
Bulletin of the Chemical Society of Japan, 2005 , vol. 78, # 2 p. 284 - 287
反应条件
1: pyridine
2: AlCl3
View Scheme
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
反应条件
aluminium trichloride
T=120°C;
参考文献
Chhaya et al.
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, 1958 , vol. 26/5 A, p. 22,26
