反应条件
1: 1.) Mg / 1.) THF, 3 h (adding), then RT, 3 h, 2.) THF, -40 deg C, 3 h (adding), -15 deg C, 1 h, then RT
2: 92.7 percent / FeCl3-SiO2 / 3 h / Ambient temperature
View Scheme
参考文献
Fadel, A.; Salaun, J.
Tetrahedron, 1985 , vol. 41, # 7 p. 1267 - 1276
