1,3-双(苄氧基)-2-丙醇合成路线 (共 35 条)
反应条件
sodium hydroxide; benzyl alcohol T=140 - 150°C;
参考文献
Journal of the Chemical Society, , p. 449
Chemistry and Industry (London, United Kingdom), , p. 1022
反应条件
diisobutylaluminium hydride in toluene 5 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemistry Letters, , p. 1593 - 1596
反应条件
sodium hydride 1.) DMF, 0 deg C, 2.) DMF, 120 deg C, 16 h; Yield given. Multistep reaction;
参考文献
Organic Preparations and Procedures International, , vol. 25, # 6 p. 639 - 647
反应条件
di(n-butyl)tin oxide; cesium fluoride 1) toluene, 1 h, reflux, 2) DMF, r.t., 10 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 39, # 8 p. 1972 - 1982
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 25, p. 823 - 827
反应条件
di(n-butyl)tin oxide; cesium fluoride multistep reaction; reaction with benzyl bromide; effect of differnt amounts of benzyl halides and CsF; effect of different reaction times and temperatures; Product distribution;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 39, # 8 p. 1972 - 1982
反应条件
(i) NaNH2, (ii) ethyl halide, (iii) H2, Pd-C; Multistep reaction;
参考文献
Berecoechea,J.; Anatol,J.
Comptes Rendus des Seances de l'Academie des Sciences, Serie C: Sciences Chimiques, 1969 , vol. 268, p. 434 - 437
反应条件
palladium dihydroxide
参考文献
Nemoto, Hisao; Wilson, J. Gerald; Nakamura, Hiroyuki; Yamamoto, Yoshinori
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 435
反应条件
tetra-(n-butyl)ammonium iodide; sodium hydride 1.) THF, 0 deg C, 2.) THF, RT, 12 h; Yield given. Multistep reaction;
参考文献
Chong, J. Michael; Sokoll, Kenneth K.
Organic Preparations and Procedures International, 1993 , vol. 25, # 6 p. 639 - 647
反应条件
hydrogenchloride in dichloromethane
T=0°C; 3 h;
参考文献
Singh, P. K.; Saluja, Sunita; Pratap, Ram; George, C. X.; Bhakuni, D. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 823 - 827