1,3-双(苄氧基)-2-丙醇合成路线 （共 35 条）
反应条件
chromium dichloride; lithium iodide in water; ethyl acetate T=75°C; 8 h;
参考文献
Falck; Barma; Baati, Rachid; Mioskowski, Charles
Angewandte Chemie - International Edition, 2001 , vol. 40, # 7 p. 1281 - 1283
反应条件
potassium hydroxide; tetra-(n-butyl)ammonium iodide in water T=60 - 70°C; 40 h;
参考文献
Nemoto, Hisao; Wilson, J. Gerald; Nakamura, Hiroyuki; Yamamoto, Yoshinori
Journal of Organic Chemistry, 1992 , vol. 57, # 2 p. 435
反应条件
1: benzyl alcohol With sodium hydroxide in water 0.166667 h; 2: epichlorohydrin in water T=25°C; 16.5 h;
参考文献
ALT SOLUTIONS, INC.
Patent: WO2007/106561 A2, 2007 ;
Location in patent: Page/Page column 63 ;
反应条件
1: glycerol With di(n-butyl)tin oxide in methanol; toluene T=100°C; 3 h; Inert atmosphere; 2: benzyl bromide With tetrabutylammomium bromide; N-ethyl-N,N-diisopropylamine in toluene T=100°C; 8 h; Inert atmosphere; regioselective reaction;
参考文献
Simas, Alessandro B.C.; da Silva, Angelo A.T.; dos Santos Filho, Tarcizio J.; Barroso, Pedro T.W.
Tetrahedron Letters, 2009 , vol. 50, # 23 p. 2744 - 2746
反应条件
1: benzyl alcohol With sodium hydroxide in water T=25 - 45°C; 0.166667 - 0.25 h; 2: epichlorohydrin in water T=25 - 45°C; 22.5 - 22.6667 h;
参考文献
WO2008/155613 A1, ;
Page/Page column 11 ;
反应条件
tri-n-butyl-tin hydride; magnesium bromide in dichloromethane T=20°C; Reduction; ring cleavage; 0.166667 h;
参考文献
Zheng; Yamauchi; Dei; Kusaka; Matsui; Yonemitsu
Tetrahedron Letters, 2000 , vol. 41, # 33 p. 6441 - 6445
反应条件
in benzyl alcohol Etherification; 1.5 h; Heating;
参考文献
Doyle, Michael P.; Tedrow, Jason S.; Dyatkin, Alexey B.; Spaans, Coenraad J.; Ene, Doina G.
Journal of Organic Chemistry, 1999 , vol. 64, # 24 p. 8907 - 8915
反应条件
sodium hydride T=100°C;
参考文献
Ogilvie; Nguyen-Ba; Gillen; et al.
Canadian Journal of Chemistry, 1984 , vol. 62, # 2 p. 241 - 252
反应条件
copper acetylacetonate 4 h; Heating;
参考文献
Sirkecioglu, Okan; Karliga, Bekir; Talinli, Naciye
Tetrahedron Letters, 2003 , vol. 44, # 46 p. 8483 - 8485
反应条件
borane-THF in tetrahydrofuran 48 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 53, # 26 p. 6005 - 6009
