chlorine Irradiation;

1: (i) NaNO2, HBF4, (ii) (thermolysis) 2: Cl2 / Irradiation View Scheme

1: Sn, aq. HCl 2: (i) NaNO2, HBF4, (ii) (thermolysis) 3: Cl2 / Irradiation View Scheme

2: NaOEt / ethanol View Scheme

air; ammonia; water; V-8Ti-xO T=250°C; various temperatures, other catalyst; Product distribution;

暂无反应条件数据

1: 94.9 percent / K2CO3, <(C7-C9)3NCH3>CH3SO4 / toluene / 3 h / Heating 2: 80 percent / 30percent KOH / H2O / 8 h / Heating View Scheme

2: NaOEt / ethanol View Scheme

1.1: 90 percent / KI; K2CO3 / dimethylformamide / 4 h / 20 °C 2.1: NBS; AIBN / chlorobenzene / 1.5 h / 90 °C 3.1: 33.0 g / i-Pr2NEt / dimethylformamide / 2 h / 20 °C 4.1: 87 percent / HCl; HCO2H / 10 percent Pd/C/water / diethyl ether / 3.5 h / 20 °C / atmospheric pressure 5.1: Et3N / CH2Cl2 / 24 h / 20 °C 5.2: 71 percent / Et3N / CH2Cl2 / 3 h / 20 °C View Scheme

1.1: 90 percent / K2CO3; KI / dimethylformamide / 20 - 50 °C 2.1: 71 percent / NaNO3; H2SO4 / 0 °C 3.1: N-bromosuccinimide; 2,2'-azobis(isobutyronitrile) / CCl4 / Heating 4.1: N,N-diisopropylethylamine / dimethylformamide / 20 °C 5.1: 96 percent / aq. HCl; Fe / ethanol / 0 °C 6.1: 98 percent / Et3N / CH2Cl2 / 1 h / 20 °C 7.1: Me3Al; N,N-diisopropylethylamine / CH2Cl2; hexane / 0 °C 7.2: 94 percent / CH2Cl2; hexane / 0 °C 8.1: 75 percent / dioxane / 0 °C 9.1: 79 percent / aq. NaOH / methanol / 1 h / 60 °C View Scheme