aluminium trichloride in dichloromethane ice-cooling;

T=50°C; Rate constant;

aluminium trichloride in dichloromethane ice-cooling;

1: 68 percent / ethanol; CCl4 / 48 h / -10 °C 2: 98 percent / H2 / 5percent Pd/C / methanol / 7 h / 760 Torr 3: 80 percent / Na2CO3 / CHCl3; H2O / 1.) 0 deg C, 30 min, 2.) RT, 2h 4: 12 percent / SOCl2 / CHCl3 / 48 h / Ambient temperature 5: 78 percent / potassium tert-butoxide / benzene; hexamethylphosphoric acid triamide / 2 h / Ambient temperature 6: 72 percent / LiALH4 / tetrahydrofuran / 24 h / Ambient temperature View Scheme

Product distribution;

Sonnenlicht; unter Ausschluss von Luft.Irradiation;

暂无反应条件数据

Hydrogenation;

暂无反应条件数据

暂无反应条件数据