1: With dihydrogen peroxide in chloroform T=-20°C; 16 h; 2: With N-ethyl-N,N-diisopropylamine in chloroform T=30°C; 15 h; Further stages. Title compound not separated from byproducts.;
1: With dimethylsulfide borane complex in tetrahydrofuran 1.08333 h; 2: With sodium tetrahydroborate in tetrahydrofuran T=20°C; Cooling with ice; 3: With toluene-4-sulfonic acid in tetrahydrofuran; ethanol T=20°C; 0.583333 h;
参考文献
Bode, Moira L.; Gates, Paul J.; Gebretnsae, Samson Y.; Vleggaar, Robert
Tetrahedron, 2010 , vol. 66, # 11 p. 2026 - 2036
