二乙基(2Z)-2-甲基-2-丁烯二酸酯合成路线 (共 42 条)
反应条件
sodium hydroxide; sodium metasilicate; diethylenetriamine-N,N,N',N'',N''-pentaacetic acid; dihydrogen peroxide
1.) water, 25 deg C, 60 min, pH 9.0, 2) methylene chloride, reflux, 2 h; Multistep reaction;
参考文献
Gellerstedt, Goeran; Hardell, Hanne-Lise; Lindfors, Eva-Lisa
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1980 , vol. 34, # 9 p. 669 - 674
参考文献
Perkin
Journal of the Chemical Society, 1888 , vol. 53, p. 576
Journal of the Chemical Society, 1896 , vol. 69, p. 1237
反应条件
Gleichgewichtsgemisch;
参考文献
Coulson; Kon
Journal of the Chemical Society, 1932 , p. 2571
参考文献
Coulson; Kon
Journal of the Chemical Society, 1932 , p. 2571
参考文献
Coulson; Kon
Journal of the Chemical Society, 1932 , p. 2571
参考文献
Hope
Journal of the Chemical Society, 1912 , vol. 101, p. 893
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Ingold; Shoppee; Thorpe
Journal of the Chemical Society, 1926 , p. 1484
反应条件
1: sodium ethylate
2: sodium; alcohol / 80 °C
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参考文献
Ingold; Shoppee; Thorpe
Journal of the Chemical Society, 1926 , p. 1484
参考文献
Ingold; Shoppee; Thorpe
Journal of the Chemical Society, 1926 , p. 1484
反应条件
T=80°C; Prod.5:Cyclopentanon-(3)-tricarbonsaeure-(1.2.4)-triaethylester,Prod.6:Cyclopentanon-(1)-dicarbonsaeure-(2.3 oder 2.4)-diaethylester usw.;
参考文献
Ingold; Shoppee; Thorpe
Journal of the Chemical Society, 1926 , p. 1484
参考文献
Hope
Journal of the Chemical Society, 1912 , vol. 101, p. 893
Show Details
Michael
Chemische Berichte, 1900 , vol. 33, p. 3756
Chemische Berichte, 1903 , vol. 36, p. 763