二乙基(2Z)-2-甲基-2-丁烯二酸酯合成路线 (共 42 条)
反应条件
lithium hydroxide in tetrahydrofuran T=20°C; 8 h; Inert atmosphere;
参考文献
Sharma, Vasudha; Kelly, Gilbert T.; Watanabe, Coran M. H.
Organic Letters, 2008 , vol. 10, # 21 p. 4815 - 4818
参考文献
Hope
Journal of the Chemical Society, 1912 , vol. 101, p. 893
反应条件
1: NADP; Old Yellow Enzyme 1; water / dimethyl sulfoxide; aq. phosphate buffer / 24 h / 30 °C / pH 7.0 / |Enzymatic reaction 2: sulfuric acid / |Reflux View Scheme
参考文献
Brenna, Elisabetta; Gatti, Francesco G.; Manfredi, Alessia; Monti, Daniela; Parmeggiani, Fabio
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 14-15 p. 2859 - 2864
参考文献
Ingold; Shoppee; Thorpe
Journal of the Chemical Society, 1926 , p. 1484
反应条件
T=80°C; Prod.5:Cyclopentanon-(3)-tricarbonsaeure-(1.2.4)-triaethylester,Prod.6:Cyclopentanon-(1)-dicarbonsaeure-(2.3 oder 2.4)-diaethylester usw.;
参考文献
Ingold; Shoppee; Thorpe
Journal of the Chemical Society, 1926 , p. 1484
参考文献
Coulson; Kon
Journal of the Chemical Society, 1932 , p. 2571
反应条件
Prod.5:Cyclopentanon-(3)-tricarbonsaeure-(1.2.4)-triaethylester, usw.;
参考文献
Ingold; Shoppee; Thorpe
Journal of the Chemical Society, 1926 , p. 1484
反应条件
Prod.5:Cyclopentanon-(3)-tricarbonsaeure-(1.2.4)-triaethylester,Prod.6:Cyclopentanon-(1)-dicarbonsaeure-(2.3 oder 2.4)-diaethylester usw.;
参考文献
Ingold; Shoppee; Thorpe
Journal of the Chemical Society, 1926 , p. 1484
参考文献
Ingold; Shoppee; Thorpe
Journal of the Chemical Society, 1926 , p. 1484
反应条件
1: sodium ethylate 2: sodium; diethyl ether View Scheme
参考文献
Ingold; Shoppee; Thorpe
Journal of the Chemical Society, 1926 , p. 1484