2,3-二氯-5-三氟甲基吡啶合成路线 （共 43 条）
反应条件
iron(III) chloride in water
反应条件
SbF3 0.166667 h; HeatingIrradiation;
参考文献
Haga, Takahiro; Fujikawa, Kan-ichi; Koyanagi, Tohru; Nakajima, Toshio; Hayashi, Kouji
Heterocycles, 1984 , vol. 22, # 1 p. 117 - 124
反应条件
FeCl3 in (2S)-N-methyl-1-phenylpropan-2-amine hydrate
反应条件
copper(l) chloride in acetonitrile T=190°C; 0.5 h;
参考文献
Martin, Pierre; Steiner, Eginhard; Streith, Jacques; Winkler, Tammo; Bellus, Daniel
Tetrahedron, 1985 , vol. 41, # 19 p. 4057 - 4078
反应条件
antimony(V) pentachloride
反应条件
1: (p-chlorophenyl)acetonitrile With Sodium hydride in N,N-dimethyl-formamide 0.25 h; NaH in DMF was mixed with DMF-soln. of CN-compd. within 20 minStirring; 2: 2,3-dichloro-5-(trifluoromethyl)-pyridine 0.333333 h; CF3-compd. was added dropwise within 20 min;
参考文献
BASF Aktiengesellschaft
Patent: US6337305 B1, 2002 ;
Location in patent: Example 1 ;
反应条件
potassium carbonate in ethanol T=60 - 90°C; 8.5 h;
参考文献
Haga, Takahiro; Fujikawa, Kan-ichi; Koyanagi, Tohru; Nakajima, Toshio; Hayashi, Kouji
Heterocycles, 1984 , vol. 22, # 1 p. 117 - 124
反应条件
ammonium hydroxide T=100 - 125°C; P=1520 Torr; 29 h;
参考文献
Haga, Takahiro; Fujikawa, Kan-ichi; Koyanagi, Tohru; Nakajima, Toshio; Hayashi, Kouji
Heterocycles, 1984 , vol. 22, # 1 p. 117 - 124
