2-(溴甲基)-6-甲基吡啶合成路线 （共 11 条）
反应条件
sulfuric acid; hydrogen bromide 12 h; Heating;
参考文献
Feig, Andrew L.; Lippard, Stephen J.
Journal of the American Chemical Society, 1994 , vol. 116, # 18 p. 8410 - 8411
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 7 h; Reflux;
参考文献
Li, Wei; Xie, Jian-Hua; Lin, Han; Zhou, Qi-Lin
Green Chemistry, 2012 , vol. 14, # 9 p. 2388 - 2390
反应条件
1: 91.5 percent / NaBH4 / ethanol / 0 °C 2: 82.5 percent / 40percent H2SO4, 60percent HBr / 12 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 116, # 18 p. 8410 - 8411
反应条件
tetrachloromethane; N-bromosuccinmide; dibenzoyl peroxide
参考文献
Journal of the American Chemical Society, , vol. 75, p. 3830
反应条件
diethyl ether anschliessend Behandeln mit Brom;
参考文献
Journal of the American Chemical Society, , vol. 75, p. 3830
反应条件
1: diethyl ether; lithium alanate 2: aqueous hydrobromic acid View Scheme
参考文献
Journal of the Chemical Society, , p. 3594,3601
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran; acetonitrile 0.25 h; Heating / reflux;
参考文献
PIRAMED LIMITED; THE INSTITUTE OF CANCER RESEARCH
Patent: WO2008/125839 A2, 2008 ;
Location in patent: Page/Page column 44 ;
WO 2008/125839 A2
反应条件
in acetonitrile T=20°C; RefluxInert atmosphere;
参考文献
Vyvyan, James R.; Brown, Rebecca C.; Woods, Brian P.
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1374 - 1376
反应条件
T(p-NO2)PPFeCl; [bis(acetoxy)iodo]benzene; water in methanol T=50°C; 12 h;
参考文献
Zhong, Qi-Di; Xue, Yun-Zhou; Yan, Hong; Song, Xiu-Qing; Zhong, Ru-Gang
Bioorganic and Medicinal Chemistry Letters, 2010 , vol. 20, # 18 p. 5532 - 5535
反应条件
sodium hydroxide in water Heating;
参考文献
Feig, Andrew L.; Lippard, Stephen J.
Journal of the American Chemical Society, 1994 , vol. 116, # 18 p. 8410 - 8411
