3,6-二苯基-1,2,4,5-四嗪合成路线 (共 59 条)
反应条件
acetic acid; sodium nitrite in diethyl ether T=20°C; 5 h;
参考文献
Rao, Guo-Wu; Hu, Wei-Xiao
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 14 p. 3702 - 3705
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran Reflux;
参考文献
Liu, Haixuan; Wei, Yunyang
Tetrahedron Letters, 2013 , vol. 54, # 35 p. 4645 - 4648
反应条件
ethanol; hydrazine hydrate
参考文献
Chemische Berichte, , vol. 45, p. 2732
反应条件
in benzonitrile T=150°C;
参考文献
Myznikov; Artamonova; Bel'skii; Stash; Skvortsov; Koldobskii
Russian Journal of Organic Chemistry, 2002 , vol. 38, # 9 p. 1360 - 1369
反应条件
1: With NH2NH2•xH2O; sulfur in ethanol T=24.84°C; Inert atmosphereReflux; 2: With acetic acid; sodium nitrite in diethyl ether; water 4 h;
参考文献
Hu, Wei-Xiao; Xu, Feng
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 6 p. 1745 - 1750
反应条件
1: With NH2NH2•xH2O; sulfur in ethanol T=24.84°C; Inert atmosphereReflux; 2: With acetic acid; sodium nitrite in diethyl ether; water 4 h;
参考文献
Hu, Wei-Xiao; Xu, Feng
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 6 p. 1745 - 1750
反应条件
in chloroform 1008 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2709 - 2712
反应条件
hydrazine monohydrochloride; triethylamine in tetrahydrofuran; dichloromethane Further byproducts given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2184 - 2190
反应条件
1: 93 percent / tetrabutylammonium bromide; aq. sodium hydroxide / CHCl3 / 20 °C 2: 65 percent / benzonitrile / 150 °C View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 38, # 9 p. 1360 - 1369
反应条件
1: triethylamine / CH2Cl2 2: hydrazinium chloride, triethylamine / CH2Cl2; tetrahydrofuran View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2184 - 2190