4-环戊基-3-氧代丁酸乙酯合成路线 （共 7 条）
反应条件
pyridinium chlorochromate in dichloromethane Ambient temperature;
参考文献
Cane; Thomas
Journal of the American Chemical Society, 1984 , vol. 106, # 18 p. 5295 - 5303
反应条件
1: propanedioic acid monoethyl ester With n-butyllithium in tetrahydrofuran; hexane T=-78 - -10°C; 2: 2-cyclopentylacetyl chloride in tetrahydrofuran; hexane T=-78°C; 0.166667 h; Further stages.;
参考文献
Lager, Erik; Nilsson, Jakob; stergaard Nielsen, Elsebet; Nielsen, Mogens; Liljefors, Tommy; Sterner, Olov
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 14 p. 6936 - 6948
反应条件
1: lithium aluminium hydride / tetrahydrofuran / 2 h / Heating 2: pyridinium chlorochromate / CH2Cl2 / Ambient temperature 3: n-butyllithium, diisopropylamine / tetrahydrofuran / -90 °C 4: 79 percent / pyridinium chlorochromate / CH2Cl2 / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 106, # 18 p. 5295 - 5303
反应条件
1: pyridinium chlorochromate / CH2Cl2 / Ambient temperature 2: n-butyllithium, diisopropylamine / tetrahydrofuran / -90 °C 3: 79 percent / pyridinium chlorochromate / CH2Cl2 / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 106, # 18 p. 5295 - 5303
反应条件
1: n-butyllithium, diisopropylamine / tetrahydrofuran / -90 °C 2: 79 percent / pyridinium chlorochromate / CH2Cl2 / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 106, # 18 p. 5295 - 5303
反应条件
diethyl ether Einleiten von Ammoniak in eine aether. Loesung des Reaktionsprodukts;
反应条件
potassium hydroxide; water
参考文献
Bulletin de la Societe Chimique de France, , p. 600,606
Journal of the American Chemical Society, , vol. 78, p. 1485,1491
