4-(3-溴丙氧基)-苯酚合成路线 （共 3 条）
反应条件
hydrogen; palladium 10 on activated carbon in tetrahydrofuran
P=2068.65 Torr;
参考文献
Butler, Christopher R.; Edwards, James P.; Fourie, Anne M.; Grice, Cheryl A.; Karlsson, Lars; Savall, Brad M.; Tays, Kevin L.; Wei, Jianmei
Patent: US2006/223792 A1, 2006 ;
Location in patent: Page/Page column 23 ;
US 20060223792 A1
反应条件
potassium hydroxide in methanol
T=70°C; 12 h;
参考文献
CINCINNATI CHILDREN'S HOSPITAL MEDICAL CENTER; UNIVERSITY OF CINCINNATI; Merino, Edward J.; Mulloy, James C.; Li, Guorui; Bell-Horwath, Tiffany
Patent: US2013/230542 A1, 2013 ;
Location in patent: Paragraph 0142 ;
反应条件
1: 88 percent / aq. K2CO3 / Bu4NBr / Heating
2: 86 percent / H2 / Pd/C / methanol / 20 °C / 2844.31 Torr
View Scheme
参考文献
Ekambome Bassene, Carine; Suzenet, Franck; Hennuyer, Nathalie; Staels, Bart; Caignard, Daniel-Henri; Dacquet, Catherine; Renard, Pierre; Guillaumet, Gerald
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 17 p. 4528 - 4532
