6-溴-1-苯基磺酰基-1H-吲哚合成路线 (共 3 条)
反应条件
1: With sodium hydride in tetrahydrofuran; mineral oil T=0 - 20°C; 0.166667 h; 2: in tetrahydrofuran; mineral oil T=20°C; 2 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 22, # 5 p. 1708 - 1725
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane T=0 - 20°C; 3 h;
参考文献
Janosik, Tomasz; Shirani, Hamid; Wahlstroem, Niklas; Malky, Ilham; Stensland, Birgitta; Bergman, Jan
Tetrahedron, 2006 , vol. 62, # 8 p. 1699 - 1707
反应条件
1: 59 percent / K2CO3 / PdCl2(PPh3)2 / dimethylformamide; H2O / 100 °C 2: 99 percent / Mg / methanol View Scheme
参考文献
Sasaki, Tomomitsu; Igarashi, Yasuhiro; Ogawa, Mio; Furumai, Tamotsu
Journal of Antibiotics, 2002 , vol. 55, # 11 p. 1009 - 1012