1-(1-环己烯-1-基磺酰基)-4-甲基苯合成路线 （共 32 条）
反应条件
sodium hydride in tetrahydrofuran
T=20°C; 15 h;
参考文献
Chawla, Ruchi; Singh, Atul K.; Yadav, Lal Dhar S.
Tetrahedron, 2013 , vol. 69, # 6 p. 1720 - 1724
反应条件
1: p-toluenesulfinic acid sodium salt With polystyrene-supported-SeCl in N,N-dimethyl-formamide
T=20°C; 6 h; solid-phase reaction;
2: cyclohexene With 2,2'-azo-bisisobutyronitrile in benzene
20 h; Heating;
3: With dihydrogen peroxide in tetrahydrofuran
T=20°C; 2 h;
参考文献
Qian; Huang
Synlett, 2001 , # 12 p. 1913 - 1916
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
0.0833333 h;
参考文献
Back, Thomas G.; Collins, Scott
Journal of Organic Chemistry, 1981 , vol. 46, # 16 p. 3249 - 3256
反应条件
1: 80 percent / CCl4 / Irradiation
2: 1) 30percent H2O2, 2) NEt3 / 1) THF, -20 deg C, 2 h, 2) RT, 12 h
View Scheme
参考文献
Gancarz, Roman A.; Kice, John L.
Journal of Organic Chemistry, 1981 , vol. 46, p. 4899 - 4906
反应条件
potassium dihydrogenphosphate; tris(dibenzylideneacetone)dipalladium (0); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in toluene
T=110°C; 18 h;
参考文献
Reeves, Diana C.; Rodriguez, Sonia; Lee, Heewon; Haddad, Nizar; Krishnamurthy, Dhileep; Senanayake, Chris H.
Tetrahedron Letters, 2009 , vol. 50, # 24 p. 2870 - 2873
反应条件
triethylamine in benzene
48 h; Ambient temperature;
参考文献
Liu, Lilian Kao; Chi, Y.; Jen, Kwan-Yue
Journal of Organic Chemistry, 1980 , vol. 45, # 3 p. 406 - 410
反应条件
triethylamine in benzene
0.25 h; Ambient temperature;
参考文献
Liu, Lilian Kao; Chi, Y.; Jen, Kwan-Yue
Journal of Organic Chemistry, 1980 , vol. 45, # 3 p. 406 - 410
反应条件
ammonium cerium(IV) nitrate; sodium iodide in acetonitrile
T=0°C; 0.75 h;
参考文献
Nair, Vijay; Augustine, Anu; Suja
Synthesis, 2002 , # 15 p. 2259 - 2265
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
0.25 h; Ambient temperature; Yield given;
参考文献
Inomata, Katsuhiko; Kobayashi, Toshifumi; Sasaoka, Shin-ichi; Kinoshita, Hideki; Kotake, Hiroshi
Chemistry Letters, 1986 , p. 289 - 292
反应条件
1: aq. H2O2
2: (reduction)
3: Py
4: piperidine, piperidine*HCl / dimethylformamide / 30 °C
View Scheme
参考文献
Jones,W.M. et al.
Journal of the American Chemical Society, 1967 , vol. 89, # 2 p. 318 - 329
