2,4-二甲基-1-甲氧基苯合成路线 （共 47 条）
反应条件
1: aqueous KMnO4 2: concentrated hydriodic acid / 135 °C View Scheme
参考文献
Jacobsen
Chemische Berichte, 1878 , vol. 11, p. 900
Chemische Berichte, 1880 , vol. 13, p. 1554
反应条件
1: 13.8 percent / CH2Cl2 / 3 h / 20 °C / Irradiation 2: silica gel / rearrangement during chromatography View Scheme
参考文献
Butts, Craig P.; Eberson, Lennart; Hartshorn, Michael P.; Robinson, Ward T.; Timmerman-Vaughan, David J.
Acta Chemica Scandinavica, 1997 , vol. 51, # 1 p. 73 - 87
反应条件
in dichloromethane T=20°C; 3 h; Irradiation; Further byproducts given;
参考文献
Acta Chemica Scandinavica, , vol. 51, # 1 p. 73 - 87
反应条件
in dichloromethane T=-78°C; 3 h; Irradiationalso at 20, -20, -50 deg C; in acetonitrile at 20, -20 deg C; Product distribution;
参考文献
Acta Chemica Scandinavica, , vol. 51, # 1 p. 73 - 87
反应条件
carbon disulfide; aluminium trichloride
参考文献
Chemische Berichte, , vol. 61, p. 1502
反应条件
lithium; ethylenediamine in tetrahydrofuran T=-10°C; 5 h;
参考文献
Shindo, Takeyuki; Fukuyama, Yasuaki; Sugai, Takeshi
Synthesis, 2004 , # 5 p. 692 - 700
参考文献
Buu-Hoi et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1955 , vol. 240, p. 2241
反应条件
titanium tetrachloride in dichloromethane
参考文献
Takeda Chemical Industries, Ltd.
Patent: US6248766 B1, 2001 ;
反应条件
1: aqueous KMnO4 2: diethyl ether View Scheme
参考文献
Sprengling; Freeman
Journal of the American Chemical Society, 1950 , vol. 72, p. 1982,1983
反应条件
potassium permanganate
参考文献
Jacobsen
Chemische Berichte, 1878 , vol. 11, p. 900
Chemische Berichte, 1880 , vol. 13, p. 1554
Full Text Show Details
Sprengling; Freeman
Journal of the American Chemical Society, 1950 , vol. 72, p. 1982,1983
