2,4-二甲基-1-甲氧基苯合成路线 (共 47 条)
反应条件
potassium hydroxide; hydrazine hydrate; diethylene glycol
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 240, p. 2241
反应条件
trifluoroacetic acid 1 h; Yield given;
参考文献
Canadian Journal of Chemistry, , vol. 64, p. 1093 - 1101
反应条件
n-butyllithium; potassium tert-butylate 1.) heptane, hexane, reflux, 20 h, 2.) THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 51, # 9 p. 1432 - 1434
反应条件
n-butyllithium; potassium tert-butylate 1.) heptane, hexane, reflux, 18 h, 2.) THF, 0 deg C, 18 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 52, # 20 p. 4605 - 4608
反应条件
n-butyllithium; potassium tert-butylate 1.) heptane, hexane, reflux, 18 h, 2.) THF, 0 deg C, 18 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 52, # 20 p. 4605 - 4608
反应条件
n-butyllithium; potassium tert-butylate 1.) heptane, hexane, reflux, 18 h, 2.) THF, 0 deg C, 18 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 52, # 20 p. 4605 - 4608
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine; nickel Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 46, # 3 p. 861 - 884
反应条件
1: POCl3 2: N2H4+H2O; KOH; diethylene glycol View Scheme
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 240, p. 2241
反应条件
1: diethyl ether; aqueous HCl 2: Erhitzen unter Normaldruck auf Siedetemperatur View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. <5> 4, p. 1468,1470
反应条件
1: platinum; ethanol / Hydrogenolyse 2: glacial acetic acid 3: platinum; ethanol / Hydrogenolyse View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. <5> 6, p. 1025,1033