2-羟基-4-甲氧基苯甲醛合成路线 （共 227 条）
反应条件
zinc oxide nanoparticle
T=120°C; Knoevenagel condensation; P=7200.72 Torr; 0.1 h; Microwave irradiationNeat (no solvent);
参考文献
Kumar, B Vinay; Naik, Halehatty S. Bhojya; Girija; Kumar, B Vijaya
Journal of Chemical Sciences, 2011 , vol. 123, # 5 p. 615 - 621
反应条件
anhydrous iron chloride in ethanol
T=80°C; 24 h; Mechanism;
参考文献
He, Xinwei; Yan, Zhenglei; Hu, Xiaoqian; Zuo, Yin; Jiang, Chang; Jin, Lei; Shang, Yongjia
Synthetic Communications, 2014 , vol. 44, # 10 p. 1507 - 1514
反应条件
piperidine in ethanol
T=20°C; 3 h;
参考文献
Volmajer, Julija; Toplak, Renata; Leban, Ivan; Le Marechal, Alenka Majcen
Tetrahedron, 2005 , vol. 61, # 29 p. 7012 - 7021
反应条件
anhydrous iron chloride
T=80°C; 24 h; Mechanism;
参考文献
He, Xinwei; Yan, Zhenglei; Hu, Xiaoqian; Zuo, Yin; Jiang, Chang; Jin, Lei; Shang, Yongjia
Synthetic Communications, 2014 , vol. 44, # 10 p. 1507 - 1514
反应条件
pyridine in dichloromethane
T=20°C; 1 h;
参考文献
Sakai, Haruka; Hirano, Tomoya; Mori, Shuichi; Fujii, Shinya; Masuno, Hiroyuki; Kinoshita, Marie; Kagechika, Hiroyuki; Tanatani, Aya
Journal of Medicinal Chemistry, 2011 , vol. 54, # 20 p. 7055 - 7065
反应条件
sodium tetrahydroborate in methanol
0.0833333 h; Ambient temperature;
参考文献
Wu, Jinn; Beal, Jack L.; Doskotch, Raymond W.
Journal of Organic Chemistry, 1980 , vol. 45, # 2 p. 208 - 212
反应条件
bromine; acetic acid; mercury(II) diacetate in ethanol; hexane; chloroform
参考文献
Chaplin, David J.; Garner III, Charles Manly; Kane, Robert Ronald; Pinney, Kevin G.; Prezioso, Joseph Anthony; Edvardsen, Klaus
Patent: US2003/149003 A1, 2003 ;
反应条件
1: With AlCl3, aluminium chloride in dichloromethane
T=-20°C; 0.25 h; Inert atmosphere;
2: With bromine in dichloromethane
T=-20 - 20°C; 0.333333 h; Inert atmosphere; regioselective reaction;
参考文献
Schmidt, Bernd; Krehl, Stefan; Kelling, Alexandra; Schilde, Uwe
Journal of Organic Chemistry, 2012 , vol. 77, # 5 p. 2360 - 2367
反应条件
pyridine; pyridinium hydrobromide perbromide
T=50°C; 2 h;
参考文献
Cordoba, Ruben; Tormo, Nelida Salvador; Medarde, Antonio Fernandez; Plumet, Joaquin
Bioorganic and Medicinal Chemistry, 2007 , vol. 15, # 15 p. 5300 - 5315
参考文献
Specht, Donald P.; Martic, Peter A.; Farid, Samir; ++
Tetrahedron, 1982 , vol. 38, # 9 p. 1203 - 1211
