1-环戊基-3-苯基-1-丙酮合成路线 (共 7 条)
反应条件
1: With oxalyl dichloride; dimethyl sulfoxide in dichloromethane T=-78°C; 0.75 h; 2: With triethylamine in dichloromethane T=23°C; 0.333333 h;
参考文献
PFIZER INC.
Patent: WO2003/95441 A1, 2003 ;
Location in patent: Page/Page column 55-56 ;
反应条件
bis-triphenylphosphine-palladium(II) chloride; sodium hydrogencarbonate in 1-methyl-pyrrolidin-2-one T=140°C; Heck reaction;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 18 p. 4834 - 4838
反应条件
1: PPh3 / CH2Cl2 / 20 °C 2: tetrahydrofuran / -78 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 18 p. 4834 - 4838
反应条件
in tetrahydrofuran T=-78°C;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 18 p. 4834 - 4838
反应条件
1: diethyl ether 2: K2cr2O7; aqueous H2SO4 / 30 - 55 °C View Scheme
参考文献
Journal of the Chemical Society, , p. 1463,1464
反应条件
1: diethyl ether 2: K2cr2O7; aqueous H2SO4 / 30 - 55 °C View Scheme
参考文献
Journal of the Chemical Society, , p. 1463,1464
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 241, p. 602