反应条件
1: 1.) butyllithium / 1.) hexane, THF, -78 deg, 3h, 2.) THF, a) -78 deg, 1 h, b) RT, 0.5 h
2: sulfuric acid / methanol / 1.5 h / 0 °C
View Scheme
参考文献
Hiyama, Tamejiro; Shinoda, Masaki; Saimoto, Hiroyuki; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 9 p. 2747 - 2758
