单-6-O-(对甲苯磺酰基)-β-环糊精合成路线 (共 6 条)
反应条件
ammonia in water T=60°C; 5 h; Product distribution / selectivity;
参考文献
US2008/275139 A1, ;
Page/Page column 11 ;
反应条件
sodium hydroxide in water T=40°C; 11 h;
参考文献
Chemistry Letters, , p. 543 - 546
反应条件
T=85°C; 0.5 h; Microwave irradiation;
参考文献
Puglisi, Antonino; Spencer, John; Clarke, James; Milton, John
Journal of Inclusion Phenomena and Macrocyclic Chemistry, 2012 , vol. 73, # 1-4 p. 475 - 478
反应条件
potassium carbonate in ethanol; water
96 h; Ambient temperature;
参考文献
Nagai, Katsuyuki; Hayakawa, Kenji; Kanematsu, Ken
Journal of Organic Chemistry, 1984 , vol. 49, # 6 p. 1022 - 1027
反应条件
in N,N-dimethyl-formamide
T=50°C;
参考文献
Ueno, Akihiko; Moriwaki, Fumio; Osa, Tetsuo; Hamada, Fumio; Murai, Koichi
Tetrahedron Letters, 1985 , vol. 26, # 7 p. 899 - 902
反应条件
in N,N-dimethyl-formamide
T=65°C; 3 h; Inert atmosphere;
参考文献
Tang, Si-Ping; Hu, Ping; Chen, Huo-Yan; Chen, Sha; Mao, Zong-Wan; Ji, Liang-Nian
Journal of Molecular Catalysis A: Chemical, 2011 , vol. 335, # 1-2 p. 222 - 227