2-(三氟甲基)-1H-吡咯合成路线 (共 11 条)
反应条件
in chloroform
T=20°C; 5 h; DarknessInert atmosphere;
参考文献
Wiehn, Matthias S.; Vinogradova, Ekaterina V.; Togni, Antonio
Journal of Fluorine Chemistry, 2010 , vol. 131, # 9 p. 951 - 957
反应条件
sulfuric acid; dihydrogen peroxide; iron(II) sulfate in water; dimethyl sulfoxide
参考文献
Kino, Tatsuhito; Nagase, Yu; Ohtsuka, Yuhki; Yamamoto, Kyoko; Uraguchi, Daisuke; Tokuhisa, Kenji; Yamakawa, Tetsu
Journal of Fluorine Chemistry, 2010 , vol. 131, # 1 p. 98 - 105
反应条件
in 1,2,2-trifluoro-trichloroethane
T=-30°C; further temperature, further solvent;
参考文献
Yoshida, Masato; Yoshida, Tatsuro; Kobayashi, Michio; Kamigata, Nobumasa
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 909 - 914
反应条件
2-picoline; Na2S2O5; sulfur dioxide; zinc in N,N-dimethyl-formamide
T=65°C; P=2250.2 - 3750.3 Torr; 3 h; other pyrrole-derivatives;
参考文献
Tordeux, Marc; Langlois, Bernard; Wakselman, Claude
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 8 p. 2293 - 2299
反应条件
2,3-butadione in methanol
5 h; Irradiation;
参考文献
Umemoto, Teruo; Miyano, Osamu
Tetrahedron Letters, 1982 , vol. 23, # 38 p. 3929 - 3930
反应条件
oxygen
T=30°C; Irradiationalso in the presence of NH3, C2H4, and/or NMe3; other five-membered heteroarenes; MechanismProduct distribution;
参考文献
Bucci, Roberto; Laguzzi, Giuseppe; Pompili, Maria Luisa; Speranza, Maurizio
Journal of the American Chemical Society, 1991 , vol. 113, # 12 p. 4544 - 4550
反应条件
in tetrahydrofuran
2 h; Heating;
参考文献
Yang, Jing-Jing; Kirchmeier, Robert L.; Shreeve, Jean'ne M.
Journal of Organic Chemistry, 1998 , vol. 63, # 8 p. 2656 - 2660
反应条件
in N,N-dimethyl-formamide
6 h; Irradiation;
参考文献
Chen, Qing-Yun; Li, Zhan-Ting
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 6 p. 645 - 648
反应条件
140 h; Irradiation; Yield given;
参考文献
Naumann, Dieter; Kischkewitz, Juergen
Journal of Fluorine Chemistry, 1990 , vol. 46, # 2 p. 265 - 281
反应条件
144 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Naumann, Dieter; Kischkewitz, Juergen
Journal of Fluorine Chemistry, 1990 , vol. 46, # 2 p. 265 - 281