7-氧杂二环[4.1.0]庚烷-2-酮合成路线 (共 57 条)
反应条件
sodium hydroxide; dihydrogen peroxide; 1-(n-butyl)-3-methylimidazolium triflate in water T=25°C; 0.0833333 h;
参考文献
Limnios, Dimitris; Kokotos, Christoforos G.
Journal of Organic Chemistry, 2014 , vol. 79, # 10 p. 4270 - 4276
反应条件
tert.-butylhydroperoxide; 3 A molecular sieve; zirconium tetra-n-propoxide in dichloromethane T=-20°C; 24 h;
参考文献
Krohn, Karsten; Vinke, Ingeborg; Adam, Horst
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1467 - 1472
反应条件
4-phenylpyridine-N-oxide; iodosylbenzene; manganese(salen)-substituted polyoxometalate in dichloromethane T=24°C; 14 h;
参考文献
Adam, Waldemar; Herold, Marike; Hill, Craig L.; Saha-Moeller, Chantu R.
European Journal of Organic Chemistry, 2002 , # 5 p. 941 - 946
反应条件
urea hydrogen peroxide; methyltrioxorhenium (VII) in various solvent(s) T=20°C; Epoxidation; Oxidation; 8 h; Title compound not separated from byproducts.;
参考文献
Chemical Communications, , # 13 p. 1165 - 1166
反应条件
stainless steel; oxygen; isobutyraldehyde in carbon dioxide T=55°C; Epoxidation; Oxidation; P=142514 Torr; 18 h; Title compound not separated from byproducts.;
参考文献
Chemistry - A European Journal, , vol. 6, # 11 p. 2011 - 2015
反应条件
dihydrogen peroxide; tris(cetyl)pyridinium 12-tungstophosphate in acetonitrile T=70°C; 5 h; Product distribution; Further Variations:Catalysts;
参考文献
Journal of Chemical Research, , # 11 p. 716 - 718
反应条件
carbon dioxide; oxygen; 1-hydroxy-pyrrolidine-2,5-dione; anhydrous cobalt diacetate T=40°C; P=44734.5 Torr; 6 h; Product distribution / selectivity;
参考文献
US2008/139841 A1, ;
Page/Page column 6-7 ;
反应条件
dihydrogen peroxide; sodium hydrogencarbonate in acetonitrile T=50°C;
参考文献
European Journal of Inorganic Chemistry, , # 9 p. 1215 - 1218
反应条件
3-chloro-benzenecarboperoxoic acid; scandium tris(trifluoromethanesulfonate) in dichloromethane 3.5 h; Ambient temperature; Yield givenYields of byproduct given;
参考文献
Synlett, , # 4 p. 462 - 464
反应条件
oxygen in cyclohexane T=75°C; P=2280.15 Torr; 6 h;
参考文献
Catalysis Letters, , vol. 141, # 3 p. 432 - 437