反应条件
1: 1-(4-ethoxy-3-methoxyphenyl)-2-(2-methoxyphenoxy)-propane-1,3-diol With α,α'-azodiizobutyramidine-dihydrochloride; H218O in acetone
T=60°C; pH=5; 3 h; Inert atmosphereSodium acetate buffer;
2: N,O-bis(trimethylsilyl) trifluoroacetamide With pyridine
T=60°C; 1 h;
参考文献
Ohashi, Yasunori; Uno, Yukiko; Amirta, Rudianto; Watanebe, Takahito; Honda, Yoichi; Watanabe, Takashi
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 7 p. 2481 - 2491
