in carbon disulfide
probably formation from nearly equivalent amounts P and I2 (small excess) when dissolving in CS2 in N2 atmosphere;; removal of excess I2 at 45 to 50°C via sucking off under reduced pressure;;
参考文献
Hampton, F.
Chem. News J. Ind. Sci., 1880 , vol. 42, p. 180 - 181
Gladstone, J. H.
Philosophical Magazine (1798-1977), 1849 , vol. 35, p. 345 - 355
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Gladstone, J. H.
Journal fuer Praktische Chemie (Leipzig), 1850 , vol. 49, p. 40 - 51
in carbon disulfide
react. of a soln. of PI5 and S in CS2; formation of PI5*5S8 as intermediate; mother liquor contains I2;; intermediate not isolated;;
参考文献
Karantassis, T.
Bull. Soc. chim. France (4), 1925 , vol. 37, p. 854 - 854
