3-硝基-1,2-苯二醇合成路线 (共 38 条)
反应条件
urea hydronitrate in water; acetonitrile T=80°C; 0.5 h; Microwave irradiation; regioselective reaction;
参考文献
Verma, Sanny; Pandita, Sangeeta; Jain, Suman L.
Tetrahedron Letters, 2014 , vol. 55, # 7 p. 1320 - 1322
反应条件
formaldehyd in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; toluene
参考文献
CARTER-WALLACE INC.
Patent: EP413064 A1, 1991 ;
反应条件
nitric acid in diethyl ether 22 h; Ambient temperature;
参考文献
Journal of Organometallic Chemistry, , vol. 507, # 1-2 p. 1 - 21
反应条件
dihydrogen peroxide in acetonitrile Irradiation;
参考文献
Tetrahedron, , vol. 26, p. 255 - 265
反应条件
sulfuric acid T=135 - 140°C;
参考文献
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, , vol. <5> 21 II, p. 207
反应条件
peroxymonosulfuric acid
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 68, p. 480
参考文献
Quarterly Journal of Pharmacy and Pharmacology, , vol. 18, p. 41,43
反应条件
hydrogen bromide; acetic acid
参考文献
Journal of the Chemical Society, , p. 1681,1683
反应条件
peroxymonosulfuric acid
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 68, p. 480
反应条件
1: aqueous nitric acid; acetic acid / 30 - 35 °C 2: ethanolic KOH View Scheme
参考文献
Quarterly Journal of Pharmacy and Pharmacology, , vol. 18, p. 41,43